Passive state behavior of special austenitic and ferritic stainless steels in phosphoric acid polluted by sulfide ions
Identifieur interne : 000E92 ( Main/Exploration ); précédent : 000E91; suivant : 000E93Passive state behavior of special austenitic and ferritic stainless steels in phosphoric acid polluted by sulfide ions
Auteurs : S. El Hajjaji [France] ; L. Aries [France] ; N. Pebere [France] ; F. Dabosi [France] ; J.-P. Audouard [France] ; A. Ben Bachir [Maroc]Source :
- Corrosion : (Houston, Tex.) [ 0010-9312 ] ; 1996.
Descripteurs français
- Pascal (Inist)
English descriptors
- KwdEn :
Abstract
The passive state behavior of the ferritic Zl CD 29-4 stainless steel (SS) in industrial phosphoric acid (40 wt% H3PO4 with 1,000 ppm chloride [Cl-] and 330 ppm sulfate [SO42-]) polluted with 20 ppm sulfide ions (S2-) was compared to that of the austenitic Z2 CNDU 25-25 SS, which is known for its high corrosion resistance. Comparison was made using electrochemical techniques, electron spectroscopy for chemical analysis (ESCA), and secondary ion mass spectroscopy (SIMS). The presence of sulfide ions (S2-) increased the dissolution rate of the austenitic SS to near that of the ferritic SS. Degradation of the protective passive film on the austenitic SS was attributed to formation of compounds of nickel and copper at the expense of chromium and molybdenum. Behavior of the two SS in the passive state was not very different.
Affiliations:
- France, Maroc
- Bourgogne, Bourgogne-Franche-Comté, Midi-Pyrénées, Occitanie (région administrative), Rabat-Salé-Kénitra
- Rabat, Toulouse, le Creusot
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El Hajjaji</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Equipe de Métallurgie Physique, Laboratoire des Matériaux (URA CNRS 445), Ecole Nationale Supérieure de Chimie (INP), 118 Route de Narbonne</s1><s2>31077, Toulouse</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region">Occitanie (région administrative)</region><region type="old region">Midi-Pyrénées</region><settlement type="city">Toulouse</settlement></placeName></affiliation></author><author><name sortKey="Aries, L" sort="Aries, L" uniqKey="Aries L" first="L." last="Aries">L. Aries</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Equipe de Métallurgie Physique, Laboratoire des Matériaux (URA CNRS 445), Ecole Nationale Supérieure de Chimie (INP), 118 Route de Narbonne</s1><s2>31077, Toulouse</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region">Occitanie (région administrative)</region><region type="old region">Midi-Pyrénées</region><settlement type="city">Toulouse</settlement></placeName></affiliation></author><author><name sortKey="Pebere, N" sort="Pebere, N" uniqKey="Pebere N" first="N." last="Pebere">N. Pebere</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Equipe de Métallurgie Physique, Laboratoire des Matériaux (URA CNRS 445), Ecole Nationale Supérieure de Chimie (INP), 118 Route de Narbonne</s1><s2>31077, Toulouse</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region">Occitanie (région administrative)</region><region type="old region">Midi-Pyrénées</region><settlement type="city">Toulouse</settlement></placeName></affiliation></author><author><name sortKey="Dabosi, F" sort="Dabosi, F" uniqKey="Dabosi F" first="F." last="Dabosi">F. Dabosi</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Equipe de Métallurgie Physique, Laboratoire des Matériaux (URA CNRS 445), Ecole Nationale Supérieure de Chimie (INP), 118 Route de Narbonne</s1><s2>31077, Toulouse</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region">Occitanie (région administrative)</region><region type="old region">Midi-Pyrénées</region><settlement type="city">Toulouse</settlement></placeName></affiliation></author><author><name sortKey="Audouard, J P" sort="Audouard, J P" uniqKey="Audouard J" first="J.-P." last="Audouard">J.-P. Audouard</name><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>IRSID, Creusot Loire Industrie, CRMC, BP 56</s1><s2>71202 le Creusot</s2><s3>FRA</s3><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Bourgogne-Franche-Comté</region><region type="old region" nuts="2">Bourgogne</region><settlement type="city">le Creusot</settlement></placeName></affiliation></author><author><name sortKey="Ben Bachir, A" sort="Ben Bachir, A" uniqKey="Ben Bachir A" first="A." last="Ben Bachir">A. Ben Bachir</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>Laboratoire de Chimie Physique Appliquée, Departement de Chimie, Av Ibn, Batouta, BP 1014</s1><s2>Rabat</s2><s3>MAR</s3><sZ>6 aut.</sZ></inist:fA14><country>Maroc</country><placeName><settlement type="city">Rabat</settlement><region nuts="2">Rabat-Salé-Kénitra</region></placeName></affiliation></author></analytic><series><title level="j" type="main">Corrosion : (Houston, Tex.)</title><title level="j" type="abbreviated">Corrosion : (Houst., Tex.)</title><idno type="ISSN">0010-9312</idno><imprint><date when="1996">1996</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">Corrosion : (Houston, Tex.)</title><title level="j" type="abbreviated">Corrosion : (Houst., Tex.)</title><idno type="ISSN">0010-9312</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Austenitic stainless steel</term><term>Chemical composition</term><term>Chlorides</term><term>Comparative study</term><term>Corrosion rate</term><term>Ferritic stainless steel</term><term>Passivation</term><term>Phosphoric acid</term><term>Sulfides Ions</term><term>Surface layer</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Passivation</term><term>Etude comparative</term><term>Vitesse corrosion</term><term>Sulfure Ion</term><term>Composition chimique</term><term>Acier inoxydable austénitique</term><term>Acier inoxydable ferritique</term><term>Couche superficielle</term><term>Chlorure</term><term>Phosphorique acide</term><term>Acier Cr25Ni25Mo5Cu2</term><term>Acier Cr29Mo5</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The passive state behavior of the ferritic Zl CD 29-4 stainless steel (SS) in industrial phosphoric acid (40 wt% H<sub>3</sub>PO<sub>4</sub> with 1,000 ppm chloride [Cl<sup>-</sup>] and 330 ppm sulfate [SO<sub>4</sub><sup>2-</sup>]) polluted with 20 ppm sulfide ions (S<sup>2-</sup>) was compared to that of the austenitic Z2 CNDU 25-25 SS, which is known for its high corrosion resistance. Comparison was made using electrochemical techniques, electron spectroscopy for chemical analysis (ESCA), and secondary ion mass spectroscopy (SIMS). The presence of sulfide ions (S<sup>2-</sup>) increased the dissolution rate of the austenitic SS to near that of the ferritic SS. Degradation of the protective passive film on the austenitic SS was attributed to formation of compounds of nickel and copper at the expense of chromium and molybdenum. Behavior of the two SS in the passive state was not very different.</div></front></TEI><affiliations><list><country><li>France</li><li>Maroc</li></country><region><li>Bourgogne</li><li>Bourgogne-Franche-Comté</li><li>Midi-Pyrénées</li><li>Occitanie (région administrative)</li><li>Rabat-Salé-Kénitra</li></region><settlement><li>Rabat</li><li>Toulouse</li><li>le Creusot</li></settlement></list><tree><country name="France"><region name="Occitanie (région administrative)"><name sortKey="El Hajjaji, S" sort="El Hajjaji, S" uniqKey="El Hajjaji S" first="S." last="El Hajjaji">S. El Hajjaji</name></region><name sortKey="Aries, L" sort="Aries, L" uniqKey="Aries L" first="L." last="Aries">L. Aries</name><name sortKey="Audouard, J P" sort="Audouard, J P" uniqKey="Audouard J" first="J.-P." last="Audouard">J.-P. Audouard</name><name sortKey="Dabosi, F" sort="Dabosi, F" uniqKey="Dabosi F" first="F." last="Dabosi">F. Dabosi</name><name sortKey="Pebere, N" sort="Pebere, N" uniqKey="Pebere N" first="N." last="Pebere">N. Pebere</name></country><country name="Maroc"><region name="Rabat-Salé-Kénitra"><name sortKey="Ben Bachir, A" sort="Ben Bachir, A" uniqKey="Ben Bachir A" first="A." last="Ben Bachir">A. Ben Bachir</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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